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Synthesis and characterization of conducting copolymer of (N1,N3-bis(thiophene-3-ylmethylene)benzene-1,3-diamine-co-3,4-ethylenedioxythiophene)
Kümbül, Altuğ, Turaç, Ersen, Dursun, Tuğba and Şahmetlioğlu, Ertuğrul Synthesis and characterization of conducting copolymer of (N1,N3-bis(thiophene-3-ylmethylene)benzene-1,3-diamine-co-3,4-ethylenedioxythiophene) Chemical Papers, Vol.64, No. 1, 2010, 114-117
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Document type:
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Článok z časopisu / Journal Article |
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Collection:
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Chemical papers
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| Author(s) |
Kümbül, Altuğ
Turaç, Ersen
Dursun, Tuğba
Şahmetlioğlu, Ertuğrul
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| Title |
Synthesis and characterization of conducting copolymer of (N1,N3-bis(thiophene-3-ylmethylene)benzene-1,3-diamine-co-3,4-ethylenedioxythiophene)
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| Journal name |
Chemical Papers
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| Publication date |
2010
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| Year available |
2010
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| Volume number |
64
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| Issue number |
1
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| ISSN |
0366-6352
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| Start page |
114
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| End page |
117
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| Place of publication |
Poland
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| Publisher |
Versita
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| Collection year |
2010
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| Language |
english
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| Subject |
250000 Chemical Sciences
250500 Macromolecular Chemistry
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| Abstract/Summary |
Electrochemical copolymerization of N 1,N 3-bis(thiophene-3-ylmethylene)benzene-1,3-diamine (TMBA) with 3,4-ethylenedioxythiophene (EDOT) was carried out in a CH3CN/LiClO4 (0.1 M) solvent-electrolyte via potentiodynamic electrolysis. Chemical structure of the monomer was determined by nuclear magnetic resonance (1H NMR) and Fourier transform infrared (FTIR) spectroscopy. The resulting copolymer was characterized by cyclic voltammetry (CV), FTIR, scanning electron microscopy (SEM), and thermogravimetry analyses (TGA). Conductivity measurements of the copolymer and PEDOT (poly(3,4-ethylenedioxythiophene)) were carried out by the four-probe technique.
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