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Influence of process parameters on the epoxidation of 2-buten-1-ol over titanium silicalite TS-1 catalyst
Wróblewska, Agnieszka, Ławro, Ewelina and Milchert, Eugeniusz Influence of process parameters on the epoxidation of 2-buten-1-ol over titanium silicalite TS-1 catalyst Chemical Papers, Vol.62, No. 2, 2008, 147-153
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Document type:
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Článok z časopisu / Journal Article |
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Collection:
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Chemical papers
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| Author(s) |
Wróblewska, Agnieszka
Ławro, Ewelina
Milchert, Eugeniusz
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| Title |
Influence of process parameters on the epoxidation of 2-buten-1-ol over titanium silicalite TS-1 catalyst
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| Journal name |
Chemical Papers
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| Publication date |
2008
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| Year available |
2008
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| Volume number |
62
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| Issue number |
2
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| ISSN |
0366-6352
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| Start page |
147
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| End page |
153
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| Place of publication |
Poland
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| Publisher |
Versita
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| Collection year |
2008
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| Language |
english
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| Subject |
250000 Chemical Sciences
250300 Organic Chemistry
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| Abstract/Summary |
The influence of process parameters on the epoxidation of 2-buten-1-ol with 30 % hydrogen peroxide using the titanium silicalite TS-1 is presented. The studies were carried out under autogenic pressure (in autoclave). Methanol was used as a solvent in this process. The influence of temperature, 2-buten-1-ol to hydrogen peroxide mole ratio, amount of solvent used, TS-1 catalyst content, and reaction time on the reaction was studied. The major product of this reaction, 2,3-epoxybutan-1-ol (EB), has numerous applications in chemical industry.
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