Reactive distillation — experimental data for propyl propionate synthesis

Kotora, Marcel, Buchaly, Carsten, Kreis, Peter, Górak, Andrzej and Markoš, Jozef Reactive distillation — experimental data for propyl propionate synthesis Chemical Papers, Vol.62, No. 1, 2008, 65-69

Document type: Článok z časopisu / Journal Article
Collection: Chemical papers  

Author(s) Kotora, Marcel
Buchaly, Carsten
Kreis, Peter
Górak, Andrzej
Markoš, Jozef
Title Reactive distillation — experimental data for propyl propionate synthesis
Journal name Chemical Papers
Publication date 2008
Year available 2008
Volume number 62
Issue number 1
ISSN 0366-6352
Start page 65
End page 69
Place of publication Poland
Publisher Versita
Collection year 2008
Language english
Subject 290000 Engineering and Technology
291100 Environmental Engineering
Abstract/Summary A set of experimental data for heterogeneously catalysed esterification of propan-1-ol and propionic acid to propyl propionate in a pilot scale reactive distillation column is presented. The catalytic section of the column was equipped with the structured packing Katapak SP-11. Both, rectifying and stripping, sections consisted of the non-reactive structured Sulzer BX packing. As catalyst, the strongly acidic ion-exchange resin Amberlyst 46 was used. The experimental results show concentration as well as temperature profiles along the column height and therefore exhibit reliable data for model validation purposes.
 
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