 |
Crystal structure and thermal chemical properties of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane
Li, X. M., Ding, C. F., Tian, B. Q., Liu, Q., Zhang, S. S., Xu, H. and Ouyang, P. K. Crystal structure and thermal chemical properties of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane Chemical Papers, Vol.60, No. 3, 2006, 220-223
|
|
|
Document type:
|
Článok z časopisu / Journal Article |
|
Collection:
|
Chemical papers
|
|
| Author(s) |
Li, X. M.
Ding, C. F.
Tian, B. Q.
Liu, Q.
Zhang, S. S.
Xu, H.
Ouyang, P. K.
|
| Title |
Crystal structure and thermal chemical properties of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane
|
| Journal name |
Chemical Papers
|
| Publication date |
2006
|
| Year available |
2006
|
| Volume number |
60
|
| Issue number |
3
|
| ISSN |
0366-6352
|
| Start page |
220
|
| End page |
223
|
| Place of publication |
Poland
|
| Publisher |
Versita
|
| Collection year |
2006
|
| Language |
english
|
| Subject |
250000 Chemical Sciences
250300 Organic Chemistry
|
| Abstract/Summary |
The crystal structure of 2-(2,4-dimethylanilino)-3-methyl-6-diethylaminofluorane has been determined by single crystal X-ray diffraction method. The crystal belongs to triclinic system, space group P-1 with unit cell constants a = 11.2877(9) Å, b = 11.9539(9) Å, c = 12.2365(9) Å, α = 97.2580(10)°, β = 116.2850(10)°, γ = 106.3710(10)°, V = 1358.48(18) Å 3, Z = 2, D c = 1.234 g/cm3, μ = 0.079 mm−1, F(000) = 536, R and w(R) are 0.0718 and 0.2055, respectively, for 5239 unique reflections with 3745 observed reflections (I > 2σ(I)).
|
|
|
